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2C6M

Crystal structure of the human CDK2 complexed with the triazolopyrimidine inhibitor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2003-04-10
DetectorRIGAKU MSC
Spacegroup nameP 21 21 21
Unit cell lengths53.662, 71.702, 72.384
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution15.000 - 1.900
R-factor0.201
Rwork0.195
R-free0.27000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1b39
RMSD bond length0.018
RMSD bond angle1.564
Data reduction softwareCrystalClear
Data scaling softwared*TREK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.1.24)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.970
High resolution limit [Å]1.9001.900
Rmerge0.0400.220
Number of reflections21538
<I/σ(I)>15.12.9
Completeness [%]95.272.9
Redundancy2.33.07
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.2PEG3350, HEPES PH7.2, AMMONIUM ACETATE, VAPOR DIFFUSION HANGING DROP, ROOM TEMPERATURE, pH 7.20

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