2C6D
Aurora A kinase activated mutant (T287D) in complex with ADPNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-01-30 |
Detector | ADSC CCD |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 86.500, 86.500, 78.300 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.000 - 2.200 |
Rwork | 0.230 |
R-free | 0.28000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1atp |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | CNX (2000) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.000 | 2.250 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.040 | 0.330 |
Number of reflections | 17003 | |
<I/σ(I)> | 19.3 | 3 |
Completeness [%] | 97.1 | 83.2 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 3.8 | pH 3.80 |