Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 278 |
Detector technology | CCD |
Collection date | 1999-06-16 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 288.000, 288.000, 653.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.680 |
R-factor | 0.192 |
Rwork | 0.192 |
R-free | 0.19600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ms2 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.780 |
High resolution limit [Å] | 2.680 | 2.680 |
Rmerge | 0.160 | 0.210 |
Number of reflections | 212866 | |
Completeness [%] | 74.0 | 10 |
Redundancy | 2.5 | 1.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |