2C3W
Structure of CBM25 from Bacillus halodurans amylase in complex with maltotetraose
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 47.533, 94.553, 64.868 |
| Unit cell angles | 90.00, 104.65, 90.00 |
Refinement procedure
| Resolution | 63.250 - 1.810 |
| R-factor | 0.161 |
| Rwork | 0.158 |
| R-free | 0.20100 |
| Structure solution method | OTHER |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.975 |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.810 |
| Rmerge | 0.050 |
| Number of reflections | 47599 |
| <I/σ(I)> | 17.3 |
| Completeness [%] | 99.0 |
| Redundancy | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
