2C3V
Structure of iodinated CBM25 from Bacillus halodurans amylase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 30.198, 41.819, 68.183 |
| Unit cell angles | 90.00, 97.18, 90.00 |
Refinement procedure
| Resolution | 67.420 - 1.390 |
| R-factor | 0.204 |
| Rwork | 0.201 |
| R-free | 0.25000 |
| Structure solution method | SAD |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.893 |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.390 |
| Rmerge | 0.070 |
| Number of reflections | 28505 |
| <I/σ(I)> | 17.3 |
| Completeness [%] | 88.0 |
| Redundancy | 7.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
