2C3H

Structure of CBM26 from Bacillus halodurans amylase in complex with maltose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 32 2 1
Unit cell lengths	108.204, 108.204, 180.493
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 2.240
R-factor	0.207
Rwork	0.203
R-free	0.27900
Structure solution method	OTHER
RMSD bond length	0.018
RMSD bond angle	1.993
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.240
Rmerge	0.100
Number of reflections	55701
<I/σ(I)>	2
Completeness [%]	99.6
Redundancy	7.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1