2C37
RNASE PH CORE OF THE ARCHAEAL EXOSOME IN COMPLEX WITH U8 RNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-17 |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 207.020, 212.940, 433.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 93.250 - 2.800 |
R-factor | 0.267 |
Rwork | 0.266 |
R-free | 0.28200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2br2 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.197 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.120 | 0.540 |
Number of reflections | 211093 | |
<I/σ(I)> | 11 | 2.7 |
Completeness [%] | 93.2 | 83.2 |
Redundancy | 4.7 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 50 MM MES, 2.4 M SODIUM MALONATE, PH 7.0 |