2C2J
Crystal Structure Of The Dps92 From Deinococcus Radiodurans
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-03-21 |
| Detector | ADSC MARRESEARCH |
| Spacegroup name | P 2 3 |
| Unit cell lengths | 88.453, 88.453, 88.453 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 88.740 - 2.050 |
| R-factor | 0.179 |
| Rwork | 0.179 |
| Structure solution method | SAD |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.383 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.200 | 2.100 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Rmerge | 0.070 | 0.500 |
| Number of reflections | 14773 | |
| <I/σ(I)> | 40.4 | 5.6 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 21.1 | 18.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 0.01M MGCL2, 0.05M TRIS-HCL PH 7.5, 5% ISOPROPANOL |
