2C0M

apo form of the TPR domain of the pex5p receptor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 1
Unit cell lengths	53.470, 85.550, 88.890
Unit cell angles	71.17, 89.99, 73.43

Refinement procedure

Resolution	19.540 - 2.500
R-factor	0.265
Rwork	0.263
R-free	0.30900
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013
RMSD bond angle	1.390
Data reduction software	XDS
Data scaling software	XDS
Phasing software	MOLREP
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.600
High resolution limit [Å]	2.500	2.500
Rmerge	0.140	0.540
Number of reflections	47257
<I/σ(I)>	6.31	1.7
Completeness [%]	95.9	85.9
Redundancy	2.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1