2C0J
Crystal structure of the bet3-trs33 heterodimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6B |
Synchrotron site | PAL/PLS |
Beamline | 6B |
Temperature [K] | 110 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.877, 70.515, 88.965 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.200 |
R-factor | 0.2187 |
Rwork | 0.219 |
R-free | 0.23680 |
Structure solution method | OTHER |
RMSD bond length | 0.007 |
RMSD bond angle | 1.175 |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.060 |
Number of reflections | 15881 |
Completeness [%] | 92.1 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |