2BZV
Human Enteric Adenovirus Serotype 41 Short Fiber Head (pH8)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | I 21 3 |
| Unit cell lengths | 103.730, 103.730, 103.730 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.150 |
| R-factor | 0.124 |
| Rwork | 0.124 |
| R-free | 0.13100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2bzu |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.480 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 1.190 |
| High resolution limit [Å] | 1.150 | 1.150 |
| Rmerge | 0.080 | 0.330 |
| Number of reflections | 351024 | |
| <I/σ(I)> | 12 | 4 |
| Completeness [%] | 97.0 | 92 |
| Redundancy | 5.4 | 5.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 20% PEG3350, 0.25 M SODIUM DIHYDROGEN PHOSPHATE MONOBASIC, pH 8.00 |
