2BY6
Is radiation damage dependent on the dose-rate used during macromolecular crystallography data collection
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.262, 58.355, 66.765 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.870 - 1.300 |
R-factor | 0.106 |
Rwork | 0.105 |
R-free | 0.13900 |
Structure solution method | OTHER |
RMSD bond length | 0.018 |
RMSD bond angle | 2.437 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.370 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.060 | 0.250 |
Number of reflections | 52145 | |
<I/σ(I)> | 11.8 | 3.6 |
Completeness [%] | 98.8 | 93.4 |
Redundancy | 3.8 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 25% PEG 8000, 0.2 M AMMONIUM SULPHATE, 0.1 M TRIS-HCL PH 8.0 |