2BXF
Human serum albumin complexed with diazepam
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2002-10-27 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 |
| Unit cell lengths | 55.290, 55.780, 120.510 |
| Unit cell angles | 81.17, 90.22, 65.93 |
Refinement procedure
| Resolution | 22.590 - 2.950 |
| R-factor | 0.215 |
| Rwork | 0.215 |
| R-free | 0.26200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1e78 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.200 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 22.600 | 3.060 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.050 | 0.360 |
| Number of reflections | 27722 | |
| <I/σ(I)> | 10.8 | 2.6 |
| Completeness [%] | 96.6 | 96.8 |
| Redundancy | 1.9 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7.00 |
