2BXB
Human serum albumin complexed with oxyphenbutazone
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2002-10-15 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 55.160, 55.500, 120.510 |
Unit cell angles | 81.33, 90.52, 65.38 |
Refinement procedure
Resolution | 22.880 - 3.200 |
R-factor | 0.228 |
Rwork | 0.228 |
R-free | 0.27600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e78 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.200 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.900 | 3.370 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.070 | 0.340 |
Number of reflections | 22484 | |
<I/σ(I)> | 8 | 2.5 |
Completeness [%] | 96.8 | 97 |
Redundancy | 1.8 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | pH 7.00 |