2BX8
Human serum albumin complexed with azapropazone
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2004-02-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 |
Unit cell lengths | 54.200, 54.950, 119.903 |
Unit cell angles | 81.21, 91.07, 64.75 |
Refinement procedure
Resolution | 41.450 - 2.700 |
R-factor | 0.237 |
Rwork | 0.237 |
R-free | 0.27300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e78 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.400 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.500 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.040 | 0.300 |
Number of reflections | 32332 | |
<I/σ(I)> | 12.2 | 2.9 |
Completeness [%] | 95.6 | 95.4 |
Redundancy | 2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | pH 7.00 |