2BWM
1.8A CRYSTAL STRUCTURE OF of Psathyrella velutina LECTIN IN COMPLEX WITH METHYL 2-ACETAMIDO-1,2-DIDEOXY-1-SELENO-BETA-D-GLUCOPYRANOSIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-14 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 82.623, 105.287, 51.836 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 64.960 - 1.800 |
R-factor | 0.151 |
Rwork | 0.150 |
R-free | 0.18300 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.682 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.170 | 1.850 |
High resolution limit [Å] | 1.700 | 1.800 |
Rmerge | 0.100 | 0.440 |
Number of reflections | 42217 | |
<I/σ(I)> | 6.3 | 1.7 |
Completeness [%] | 99.0 | 98.2 |
Redundancy | 22.85 | 22.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 2.8M AMMONIUM SULPHATE,0.1M MES PH 6.5 |