2BW9
Laue Structure of L29W MbCO
Experimental procedure
| Experimental method | LAUE |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-ID-B |
| Synchrotron site | APS |
| Beamline | 14-ID-B |
| Temperature [K] | 288 |
| Detector technology | IMAGE PLATE |
| Collection date | 2003-12-20 |
| Detector | MARRESEARCH |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.870, 91.870, 46.040 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 50.000 - 1.680 |
| R-factor | 0.2156 |
| Rwork | 0.216 |
| R-free | 0.24940 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1d04 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.057 |
| Data reduction software | Precognition |
| Data scaling software | Precognition |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.700 |
| Rmerge | 0.140 |
| Number of reflections | 19905 |
| <I/σ(I)> | 14 |
| Completeness [%] | 78.1 |
| Redundancy | 5.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.8 | pH 7.80 |
