2BUA
Crystal Structure Of Porcine Dipeptidyl Peptidase IV (Cd26) in Complex With a Low Molecular Weight Inhibitor.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS |
Synchrotron site | SLS |
Temperature [K] | 100 |
Spacegroup name | P 1 |
Unit cell lengths | 62.425, 118.131, 133.317 |
Unit cell angles | 112.40, 94.98, 90.99 |
Refinement procedure
Resolution | 20.000 - 2.560 |
Rwork | 0.220 |
R-free | 0.25570 |
Structure solution method | OTHER |
RMSD bond length | 0.007 |
RMSD bond angle | 1.337 |
Refinement software | CNX (2002) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.560 |
Number of reflections | 109530 |
Completeness [%] | 97.2 |
Redundancy | 1.97 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |