Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-3 |
| Synchrotron site | ESRF |
| Beamline | ID14-3 |
| Temperature [K] | 277 |
| Detector technology | CCD |
| Collection date | 2001-04-22 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 85.104, 188.766, 117.817 |
| Unit cell angles | 90.00, 104.47, 90.00 |
Refinement procedure
| Resolution | 28.700 - 1.780 |
| R-factor | 0.229 |
| Rwork | 0.229 |
| R-free | 0.23700 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 1QLA |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.300 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 28.750 |
| High resolution limit [Å] | 1.780 |
| Rmerge | 0.100 |
| Number of reflections | 317968 |
| <I/σ(I)> | 16.5 |
| Completeness [%] | 92.3 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6 | pH 6.00 |
