2BQ4
Crystal structure of type I cytochrome c3 from Desulfovibrio africanus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-01-31 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 100.900, 46.300, 54.816 |
Unit cell angles | 90.00, 118.97, 90.00 |
Refinement procedure
Resolution | 48.220 - 1.680 |
R-factor | 0.202 |
Rwork | 0.200 |
R-free | 0.24000 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.379 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.220 | 1.750 |
High resolution limit [Å] | 1.680 | 1.680 |
Rmerge | 0.060 | 0.060 |
Number of reflections | 106337 | |
<I/σ(I)> | 20.2 | 11.3 |
Completeness [%] | 94.8 | 71.8 |
Redundancy | 3.9 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 3.2M NAH2PO4/K2HPO4 |