2BPY

HIV-1 protease-inhibitor complex

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	58.640, 87.280, 46.830
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 * - 1.900
R-factor	0.197
Rwork	0.197
RMSD bond length	0.014
RMSD bond angle	2.100
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.048 *
Total number of observations	95383 *
Number of reflections	16008 *
Completeness [%]	81.8 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	enzyme	6 (mg/ml)
2	1	drop	MES	10 (mM)
3	1	drop	dithiothreitol	1 (mM)
4	1	drop	EDTA	1 (mM)
5	1	drop		3 (mM)
6	1	reservoir		0.6 (M)
7	1	reservoir		0.1 (M)