2BMV
Apoflavodoxin from Helicobacter pylori
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ROTATING ANODE |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-10-25 |
| Detector | BRUCKER-NONIUS |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 36.610, 45.712, 86.652 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 9.000 - 2.110 |
| R-factor | 0.206 |
| Rwork | 0.200 |
| R-free | 0.28800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1fue |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.464 |
| Data reduction software | DENZO |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.300 | 2.180 |
| High resolution limit [Å] | 2.040 | 2.110 |
| Rmerge | 0.170 | 0.560 |
| Number of reflections | 9402 | |
| <I/σ(I)> | 11.8 | 1.3 |
| Completeness [%] | 98.9 | 90.4 |
| Redundancy | 5.1 | 1.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.50 |
