2BM8
CmcI-N160 apo-structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-07-21 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 93.652, 182.640, 103.236 |
Unit cell angles | 90.00, 91.05, 90.00 |
Refinement procedure
Resolution | 95.350 - 2.500 |
R-factor | 0.194 |
Rwork | 0.192 |
R-free | 0.24500 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.213 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 95.300 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.080 | 0.330 |
Number of reflections | 119750 | |
<I/σ(I)> | 25.7 | 3.4 |
Completeness [%] | 99.4 | 96.3 |
Redundancy | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.50 |