2BLI
L29W Mb deoxy
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Collection date | 2002-11-03 |
Detector | BRUKER MULTIWIRE |
Spacegroup name | P 6 |
Unit cell lengths | 91.750, 91.750, 46.180 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 1.700 |
R-factor | 0.1875 |
Rwork | 0.188 |
R-free | 0.20670 |
Structure solution method | OTHER |
RMSD bond length | 0.007 |
RMSD bond angle | 1.007 |
Data reduction software | SAINT |
Data scaling software | SAINT |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.780 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.050 | 0.260 |
Number of reflections | 99657 | |
<I/σ(I)> | 11 | 2.8 |
Completeness [%] | 85.3 | 73.1 |
Redundancy | 4.7 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.8 | 2.8 M AMMONIUMSULFAT, 25 MM TRIS, 1 MM EDTA, PH 8.0 |