2BK8
M1 domain from titin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-11-16 |
Detector | MARRESEARCH |
Spacegroup name | I 41 |
Unit cell lengths | 68.780, 68.780, 48.180 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 17.740 - 1.690 |
R-factor | 0.191 |
Rwork | 0.189 |
R-free | 0.23400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | HOMOLOGY MODEL |
RMSD bond length | 0.015 |
RMSD bond angle | 1.393 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.740 | 1.800 |
High resolution limit [Å] | 1.690 | 1.690 |
Rmerge | 0.040 | 0.410 |
Number of reflections | 24619 | |
<I/σ(I)> | 18.1 | 3.89 |
Completeness [%] | 99.6 | 100 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 2.2 M AMMONIUM SULFATE 0.1 M BIS TRIS PH 7.0 |