2BJB
Mycobacterium Tuberculosis Epsp Synthase In Unliganded State
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-02 |
Detector | MARRESEARCH |
Spacegroup name | H 3 |
Unit cell lengths | 102.864, 102.864, 99.512 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 1.800 |
R-factor | 0.164 |
Rwork | 0.162 |
R-free | 0.20500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g6t |
RMSD bond length | 0.021 |
RMSD bond angle | 1.888 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.19) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.820 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.110 | 0.810 |
Number of reflections | 36380 | |
<I/σ(I)> | 17.5 | 2.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.9 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.1 | 1.6M NA ACETATE, pH 6.10 |