2BIX
Crystal structure of apocarotenoid cleavage oxygenase from Synechocystis, Fe-free apoenzyme
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 122.928, 122.928, 205.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.140 - 2.680 |
R-factor | 0.21 |
Rwork | 0.210 |
R-free | 0.24300 |
Structure solution method | MIRAS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.173 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHARP |
Refinement software | TNT (5.6.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.800 | 2.850 |
High resolution limit [Å] | 2.680 | 2.680 |
Rmerge | 0.060 | 0.310 |
Number of reflections | 44859 | |
<I/σ(I)> | 24.5 | 7.2 |
Completeness [%] | 98.6 | 92.6 |
Redundancy | 8.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.7 | pH 5.70 |