2BGL
X-Ray structure of binary-Secoisolariciresinol Dehydrogenase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 58.510, 118.910, 132.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.800 |
R-factor | 0.201 |
Rwork | 0.201 |
R-free | 0.22100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bgk |
RMSD bond length | 0.010 |
RMSD bond angle | 4.300 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | AMoRE |
Refinement software | X-PLOR (NULL) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.060 | 0.290 |
Number of reflections | 5752 | |
<I/σ(I)> | 9.9 | 2.3 |
Completeness [%] | 99.7 | 99.3 |
Redundancy | 3.58 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | pH 8.50 |