2BFU
X-ray structure of CPMV top component
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Spacegroup name | I 2 3 |
Unit cell lengths | 311.407, 311.407, 311.407 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 4.000 |
R-factor | 0.23 |
Rwork | 0.230 |
Structure solution method | OTHER |
RMSD bond length | 0.012 |
RMSD bond angle | 1.500 |
Refinement software | X-PLOR (3.8) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 4.000 |
Rmerge | 0.110 |
Number of reflections | 39473 |
<I/σ(I)> | 6 |
Completeness [%] | 94.0 |
Redundancy | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |