2BB7
Mn Form Of E. coli Methionine Aminopeptidase In Complex With a quinolinyl sulfonamide inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-03-09 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.039, 60.416, 50.521 |
Unit cell angles | 90.00, 104.40, 90.00 |
Refinement procedure
Resolution | 17.620 - 1.700 |
R-factor | 0.19 |
Rwork | 0.187 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xnz |
RMSD bond length | 0.014 |
RMSD bond angle | 1.415 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.860 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.037 | 0.158 |
Number of reflections | 24139 | |
<I/σ(I)> | 11.5 | 4.6 |
Completeness [%] | 98.8 | 97.2 |
Redundancy | 3.6 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | PEG 20000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |