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2BB3

Crystal Structure of Cobalamin Biosynthesis Precorrin-6Y Methylase (cbiE) from Archaeoglobus fulgidus

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2004-10-28
DetectorADSC QUANTUM 315
Wavelength(s)0.97932
Spacegroup nameC 2 2 21
Unit cell lengths88.191, 88.418, 115.932
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.100 - 2.270
R-factor0.211
Rwork0.211
R-free0.27400
Structure solution methodSAD
RMSD bond length0.011
RMSD bond angle1.700
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSHARP
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]44.2102.280
High resolution limit [Å]2.2002.200
Rmerge0.0680.808
Number of reflections22771
<I/σ(I)>13.52.56
Completeness [%]97.382.2
Redundancy115.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.62950.1M Sodium Acetate, 11% PEG10K, 2% Iso-Propanol,10mM SAH, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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