2B5M
Crystal Structure of DDB1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2003-11-12 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.380, 133.834, 184.715 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.700 - 2.920 |
R-factor | 0.23472 |
Rwork | 0.232 |
R-free | 0.27725 |
Structure solution method | SAD |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.700 |
High resolution limit [Å] | 2.920 |
Number of reflections | 33473 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | PEG 4000, sodium chloride, MES, DTT, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | PEG 4000, sodium chloride, MES, DTT, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |