2B59
The type II cohesin dockerin complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.568, 52.220, 156.262 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.110 |
R-factor | 0.205 |
Rwork | 0.205 |
R-free | 0.24600 |
Structure solution method | SAD |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.059 | 0.200 |
Number of reflections | 25258 | |
<I/σ(I)> | 25.87 | 5.08 |
Completeness [%] | 97.2 | 81.4 |
Redundancy | 4.1 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.25 | AMMONIUM SULPHATE, DIOXANE, SODIUM ACETATE, pH 4.25 |