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2B3U

Human Spermine spermidine acetyltransferase K26R mutant

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X26C
Synchrotron siteNSLS
BeamlineX26C
Temperature [K]99
Detector technologyCCD
Collection date2003-06-21
DetectorADSC QUANTUM 4
Wavelength(s)0.98
Spacegroup nameP 43
Unit cell lengths74.300, 74.300, 63.300
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000 - 1.850
R-factor0.21
Rwork0.210
R-free0.24000
Structure solution methodSAD
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareSOLVE
Refinement softwareCNS (1.1)
Data quality characteristics
 Overall
Low resolution limit [Å]30.000
High resolution limit [Å]1.850
Number of reflections28155
Completeness [%]99.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6298mmPEG500, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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