2AZH
Solution structure of iron-sulfur cluster assembly protein SUFU from Bacillus subtilis, with zinc bound at the active site. Northeast Structural Genomics Consortium target SR17
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Varian | INOVA | 500 | |
| 2 | Varian | INOVA | 600 | |
| 3 | Varian | INOVA | 750 | |
| 4 | Varian | INOVA | 800 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 15N-1H HSQC, 2D 13C-1H HSQC, 3D HNCO, 3D HNCA, 3D HncoCA, 3D HNCACB, 3D HNcoCACB, 3D HcccoNH-TOCSY, 3D hCccoNH-TOCSY |
| 2 | 2 | 2 | 2D HH NOESY, 2D 13C-1H HSQC, 2D 15N-1H HSQC, 3D 15N-NOESY, 3D 13C-NOESY, 4D CC NOESY |
| 3 | 2 | 3 | 2D 13C-1H HSQC |
| 4 | 1 | 4 | 2D 15N-1H IPAP-HSQC |
| 5 | 1 | 5 | 2D 15N-1H IPAP-HSQC |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | ambient | 20 |
| 2 | 6.5 | ambient | 20 |
Conformers
| Conformers Calculated Total Number | 60 |
| Conformers Submitted Total Number | 10 |
