2AZA

STRUCTURE OF AZURIN FROM ALCALIGENES DENITRIFICANS. REFINEMENT AT 1.8 ANGSTROMS RESOLUTION AND COMPARISON OF THE TWO CRYSTALLOGRAPHICALLY INDEPENDENT MOLECULES

Replaces:  1AZA

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	75.000, 74.200, 99.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 1.800
R-factor	0.157
RMSD bond length	0.016
RMSD bond angle	2.900
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Number of reflections	21980 *
Completeness [%]	87.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	phosphate	0.1 (M)
2	1	1	ammonium sulphate	75 (%sat)