2AXU
Structure of PrgX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-03-03 |
| Wavelength(s) | 0.97940 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 92.654, 134.718, 195.930 |
| Unit cell angles | 90.00, 100.30, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.900 |
| R-factor | 0.201 |
| Rwork | 0.199 |
| R-free | 0.26600 |
| Structure solution method | ISO to Y153C |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 15.000 |
| High resolution limit [Å] | 2.900 |
| Number of reflections | 104010 |
| Completeness [%] | 99.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298 | PEG 4000, citrate-phophate , pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
