2AX3
CRYSTAL STRUCTURE OF A PUTATIVE CARBOHYDRATE KINASE (TM0922) FROM THERMOTOGA MARITIMA MSB8 AT 2.25 A RESOLUTION
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-02-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979245, 0.979078, 0.891940 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 121.264, 121.264, 153.873 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.890 - 2.270 |
Rwork | 0.159 |
R-free | 0.21800 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.572 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.890 | 28.890 | 2.380 |
High resolution limit [Å] | 2.260 | 7.150 | 2.260 |
Rmerge | 0.111 | 0.037 | 0.660 |
Number of reflections | 27157 | ||
<I/σ(I)> | 6.2 | 16.4 | 1.2 |
Completeness [%] | 99.9 | ||
Redundancy | 6.9 | 6.1 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION,SITTING DROP,NANODROP | 6.5 | 277 | 1.6M NaCl, 0.1M Cacodylate, pH 6.5, VAPOR DIFFUSION,SITTING DROP,NANODROP, temperature 277K |