2AWY
met-DcrH-Hr
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-05-07 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.7403 |
Spacegroup name | P 1 |
Unit cell lengths | 33.160, 44.846, 47.538 |
Unit cell angles | 92.76, 103.49, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.100 |
Rwork | 0.221 |
R-free | 0.28000 |
Structure solution method | MAD |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | PEG4000, CaCl2, isopropanol, Tris-HCl, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | PEG4000, CaCl2, isopropanol, Tris-HCl, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | PEG4000, CaCl2, isopropanol, Tris-HCl, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |