Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

2AW9

Superoxide dismutase with manganese from Deinococcus radiodurans

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.2
Synchrotron siteALS
Beamline8.2.2
Temperature [K]100
Detector technologyCCD
Collection date2005-06-10
DetectorADSC QUANTUM 315
Wavelength(s)1.5499
Spacegroup nameP 1 21 1
Unit cell lengths43.833, 83.499, 65.495
Unit cell angles90.00, 105.79, 90.00
Refinement procedure
Resolution62.990 - 2.700
R-factor0.1701
Rwork0.168
R-free0.21418
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1y67
RMSD bond length0.010
RMSD bond angle1.742
Data scaling softwareSCALEPACK
Phasing softwareEPMR
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]90.0002.800
High resolution limit [Å]2.7002.700
Number of reflections11594
<I/σ(I)>20.3297
Completeness [%]92.671.7
Redundancy5.64.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.5298magnesium chloride, tris-hydrochloride, PEG 4000, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon