2AV4
Crystal structure of Plasmodium yoelii thioredoxin-like protein 4A (DIM1)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-BM |
| Synchrotron site | APS |
| Beamline | 17-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-08-12 |
| Detector | MARRESEARCH |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 109.877, 109.877, 85.170 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 41.500 - 1.730 |
| R-factor | 0.20958 |
| Rwork | 0.208 |
| R-free | 0.26115 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1qgv |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.459 |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.500 | 1.860 |
| High resolution limit [Å] | 1.730 | 1.730 |
| Rmerge | 0.061 | 0.385 |
| Number of reflections | 20820 | |
| <I/σ(I)> | 11.3 | 2.28 |
| Completeness [%] | 95.4 | 91.3 |
| Redundancy | 2.9 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 295 | 1.4 M NaCl, pH 9.0, VAPOR DIFFUSION, temperature 295 K |
