2ATF
X-RAY STRUCTURE OF cysteine dioxygenase type I FROM MUS MUSCULUS MM.241056
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-08-09 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97915, 0.97933, 0.96392 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 57.550, 57.550, 122.076 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.860 - 1.750 |
R-factor | 0.18071 |
Rwork | 0.179 |
R-free | 0.21555 |
Structure solution method | MAD |
RMSD bond length | 0.020 |
RMSD bond angle | 1.764 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (refmac_5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.790 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.118 | 0.270 |
Number of reflections | 21529 | |
<I/σ(I)> | 15.888 | 5.25 |
Completeness [%] | 100.0 | 100 |
Redundancy | 14.2 | 13.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 273 | 10 MG/ML PROTEIN, 20% MPEG 5K, 0.16 M CALCIUM CHLORIDE, 0.10 M MES, pH 6.0, vapor diffusion, hanging drop, temperature 273K |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 273 | 10 MG/ML PROTEIN, 20% MPEG 5K, 0.16 M CALCIUM CHLORIDE, 0.10 M MES, pH 6.0, vapor diffusion, hanging drop, temperature 273K |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 273 | 10 MG/ML PROTEIN, 20% MPEG 5K, 0.16 M CALCIUM CHLORIDE, 0.10 M MES, pH 6.0, vapor diffusion, hanging drop, temperature 273K |