2AQN
CU/ZN superoxide dismutase from neisseria meningitidis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 96 |
| Collection date | 2000-02-07 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.08 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 99.791, 64.592, 82.730 |
| Unit cell angles | 90.00, 125.93, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.400 |
| R-factor | 0.1285 |
| Rwork | 0.129 |
| R-free | 0.19040 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2aps |
| RMSD bond length | 0.011 |
| RMSD bond angle | 0.028 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.450 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Rmerge | 0.045 | 0.252 |
| Number of reflections | 80120 | |
| <I/σ(I)> | 14.1 | 3.2 |
| Completeness [%] | 95.9 | 93.8 |
| Redundancy | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | AmSO4, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
