2AMA
Crystal structure of human androgen receptor ligand binding domain in complex with dihydrotestosterone
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-24 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.500, 66.300, 70.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.900 |
Rwork | 0.214 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2am9 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.100 |
Data reduction software | XNEMO |
Data scaling software | XSCALE |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.660 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.078 | 0.471 |
Number of reflections | 19480 | 2484 |
<I/σ(I)> | 18.39 | 3.36 |
Completeness [%] | 89.3 | 80.3 |
Redundancy | 8.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 293 | MgSO4, Pipes, pH 7.3, VAPOR DIFFUSION, HANGING DROP, temperature 293K |