2AK2

ADENYLATE KINASE ISOENZYME-2

Experimental procedure

Source type	ROTATING ANODE
Detector technology	AREA DETECTOR
Collection date	1992
Detector	SIEMENS
Spacegroup name	P 21 21 21
Unit cell lengths	44.200, 50.100, 123.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.100
R-factor	0.222
Rwork	0.222
RMSD bond length	0.010
RMSD bond angle	1.600
Data reduction software	XDS
Data scaling software	XDS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	2.100
Rmerge	0.050
Number of reflections	15064
Completeness [%]	92.0
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate