Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1994-04 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 130.660, 141.830, 53.150 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.600 |
| R-factor | 0.214 |
| Rwork | 0.214 |
| R-free | 0.27300 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.300 * |
| Data reduction software | DENZO |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 * |
| High resolution limit [Å] | 2.400 * |
| Rmerge | 0.066 |
| Total number of observations | 220712 * |
| Number of reflections | 37305 |
| Completeness [%] | 94.9 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 7.3 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | M.TaqI | 0.00065 (mM) | |
| 2 | 1 | drop | Sinefungin | 1 (mM) | can be replaced by AdoHcy |
| 3 | 1 | drop | duplex oligonucleotides | 0.1 (mM) | |
| 4 | 1 | drop | 200 (mM) | ||
| 5 | 1 | drop | Tris-HCl | 20 (mM) | |
| 6 | 1 | reservoir | PEG6000 | 2-6 (%) | |
| 7 | 1 | reservoir | 100 (mM) | ||
| 8 | 1 | reservoir | Tris-HCl | 20 (mM) |
