2A9P

Medium Resolution BeF3 bound RR02-rec

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 5.2R
Synchrotron site	ELETTRA
Beamline	5.2R
Temperature [K]	100
Detector technology	DIFFRACTOMETER
Collection date	2003-07-20
Detector	NICOLET
Spacegroup name	C 2 2 21
Unit cell lengths	74.705, 93.404, 37.611
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	58.320 - 1.820
R-factor	0.15876
Rwork	0.156
R-free	0.20590
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.020
RMSD bond angle	1.818
Data reduction software	MOSFLM
Data scaling software	CCP4 ((SCALA))
Phasing software	EPMR
Refinement software	REFMAC (5.2.0005)

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP			VAPOR DIFFUSION, SITTING DROP