2A90
Crystal Structure of the tandem WWE domain of Drosophila Deltex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2004-04-25 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9795, 0.9793, 0.9724 |
Spacegroup name | P 41 |
Unit cell lengths | 57.760, 57.760, 80.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.800 - 2.150 |
Rwork | 0.230 |
R-free | 0.24700 |
Structure solution method | MAD |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.800 | 2.280 |
High resolution limit [Å] | 2.150 | 2.150 |
Number of reflections | 27871 | |
Completeness [%] | 99.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | Sodium Acetate, Sodium Cacodylate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |