2A7H
On the Routine Use of Soft X-Rays in Macromolecular Crystallography, Part III- The Optimal Data Collection Wavelength
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 54.190, 54.190, 105.860 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.100 |
R-factor | 0.166 |
Rwork | 0.166 |
R-free | 0.23000 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.025 |
RMSD bond angle | 2.186 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.100 |
Number of reflections | 10801 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |