2A7B

On the Routine Use of Soft X-Rays in Macromolecular Crystallography, Part III- The Optimal Data Collection Wavelength

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 5.2R
Synchrotron site	ELETTRA
Beamline	5.2R
Temperature [K]	100
Spacegroup name	P 21 21 21
Unit cell lengths	33.430, 53.760, 66.770
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 1.650
R-factor	0.183
Rwork	0.182
R-free	0.22800
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.025
RMSD bond angle	2.030
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000
High resolution limit [Å]	1.650
Number of reflections	14704

Crystallization Conditions

crystal ID	method	pH	temperature	details
1